Method for removing tetranitromethane from nitric acid

Details Method for removing tetranitromethane from nitric acid Method for removing tetranitromethane from nitric acid

1995-10-24

1996-12-31

Langel, Wayne

Distillation: processes, separatory

With chemical reaction

Including step of adding catalyst or reacting material

159DIG19, 203 49, 203 98, 4233942, B01D 334

Patent

active

055890377

ABSTRACT:
Tetranitromethane and other polynitrated methanes can be effectively removed from otherwise substantially organic-free nitric acid streams through the addition of substantially organic-free concentrated sulfuric acid and by, optionally, performing secondary operations such as sparging the mixed acid stream with a gas such as nitric oxide or with an oil.

REFERENCES:
patent: 3401095 (1968-09-01), Saradzhev
patent: 4289706 (1981-09-01), Fukasawa et al.
patent: 4713232 (1987-12-01), Chin et al.
Yamato, O. Int. J. Radiat. Biol. Relat. Stud. Phys., Chem. Med. 1982/42(6), 661.
Sutton, H. C.; Seddon, W. A.; Sopchyshyn, F. C. Can. J. Chem. 1978,56, 1961.
Sutton, H. C. J. Chem. Soc. Faraday 1 1975,71, 2142.
Brown, L. H.; Geckler, R. D., "Research in Nitropolymers and their Application to solid smokeless Propellants" (no date available).
Harada, T.; Nishikido, N.; Morio, Y; Matuura, R. Bull. Chem. Soc. Jpn. 1981 4(9), 2592.
Mundy, R. A.; Gilbert, E. E. Report RAD-240.10, PI-557, ARLCD-TR-78027, AD-E400164, Order No. AD-A056244, Gov. Rep. Announce. Index (U>S.) 1978, 78(21), 250.
Isacs, N. S.; Abed, O. H. Tet. Lett. 1982, 23, 2799.
Frank, A. J.; Henglein, A. Berichte der Bunsen Gesellschaft 1976, 7, 393.
Kimura, M.; Ikeda, T.; Hara, N. Nippon Kagaku Karshi 1982, 3, 341.
Kumara, M.; Skukutani, M. Bull. Chem. Soc. Jap. 1979, 52, 2535.
Korsakov, V. G.; Kedrinskii, L. A. Elektrokhimiya 1976, 12, 1562.

Affiliated with

Also associated with

Rating

Method for removing tetranitromethane from nitric acid does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for removing tetranitromethane from nitric acid, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for removing tetranitromethane from nitric acid will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-1139306