Method for removing sulfur from superalloy articles to improve t

Metal treatment – Process of modifying or maintaining internal physical... – Heating or cooling of solid metal

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75626, 75628, 148426, 148427, 148428, 148429, C22F 110

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053445104

ABSTRACT:
Superalloy articles are made more oxidation resistant by a process which includes heating the article in an environment having a reduced pressure of inert gas and a low partial pressure of oxygen to a temperature at which the sulfur in the article diffuses out. The heat treatment is best carried out at a temperature within the range defined by the incipient melting temperature of the article and about 150.degree. C. below the incipient melting temperature of the article. Alternatively, the heat treatment may be carried out at a temperature above the gamma prime solvus temperature of the article and below the incipient melting temperature of the article. At such temperatures, sulfur readily diffuses out of the article, and a more oxidation resistant component is produced.

REFERENCES:
patent: 1710846 (1929-04-01), Smith et al.
patent: 3853540 (1974-12-01), Schlatter et al.
patent: 3891425 (1975-06-01), McCarty
patent: 4209348 (1980-06-01), Duhl et al.
patent: 4719080 (1988-01-01), Duhl et al.
patent: 4895201 (1990-01-01), DeCrescente et al.
Corrosion & Particle Erosion at High Temperatures, by V. Srinivasan and K. Vedula; "Effect of Sulfur Removal on Scale Adhesion to PWA 1480", by B. K. Tubbs and J. L. Smialek (p. 459); 1989.

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