Method for removing dissolved solids from aqueous waste streams

Chemistry: physical processes – Physical processes – Crystallization

Reexamination Certificate

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C588S405000, C588S410000

Reexamination Certificate

active

08052763

ABSTRACT:
A method for removing dissolved solids from a waste stream, such as that produced in flue gas scrubbing, through an evaporation-crystallization process operated at relatively low temperature. A waste stream is directed into an evaporator and heated at a temperature of less than 60° C. at a pressure below atmospheric pressure. The waste stream is concentrated through the evaporation process and forms a slurry stream having crystallized solids. At the low temperature of evaporation, the solids crystallize at substantially lower temperature and the solution has a substantially lower boiling point elevation than at atmospheric pressure. The slurry stream is directed to a solid-liquid separator where the crystallized solids in the slurry stream are separated, producing a solid cake and mother liquor.

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patent: 6233958 (2001-05-01), Mei et al.
patent: 6589497 (2003-07-01), Smith
patent: 6893474 (2005-05-01), Jafverstrom et al.
patent: 2007/0051513 (2007-03-01), Heins
Hofmann, G.; Schmitz, R.; Jung, H.; “Treatment of Waste Material: Flue Gas Cleaning”; pp. 3-10.
Hofmann, G.; Schmitz, R.; Jung, H.; “Operational Experience Gained in the Evaporation of Scrubber Liquors From Flue Gas Purification in the Thermal Treatment of Industrial Waste in the RZR Herten Centre”; Translation from AbfallwirtschaftsJournal 4 (1992), Nr. 12; 15 pages.

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