Method for recovering soluble protein

Chemistry: natural resins or derivatives; peptides or proteins; – Peptides of 3 to 100 amino acid residues – Separation or purification

Reexamination Certificate

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Details

C530S422000, C530S424000

Reexamination Certificate

active

06861505

ABSTRACT:
The present invention relates in providing a process for recovering a soluble protein having a higher recovery rate by suppressing the aggregation of the protein when a denaturing agent is removed from the solubilization treatment solution containing a solubilized protein; and providing a process for removing a denaturing agent from the above solubilization treatment solution in which the aggregation of the protein is suppressed. In a process for recovering a soluble protein comprising the steps of removing a denaturing agent from a solubilization treatment solution prepared by solubilizing insoluble protein aggregates using the denaturing agent, the process of the present invention is characterized by subjecting the solubilization treatment solution to a treatment of removing the denaturing agent in the presence of a dihydric to tetrahydric, polyhydric alcohol at a concentration of 60 to 99% by volume, and thereafter diluting with a diluent solution the treatment solution obtained after the removal treatment. In a process for removing a denaturing agent from a solubilization treatment solution prepared by solubilizing insoluble protein aggregates using the denaturing agent, the process of the present invention is characterized by subjecting the solubilization treatment solution to a treatment of removing the denaturing agent in the presence of a dihydric to tetrahydric, polyhydric alcohol.

REFERENCES:
patent: 0360937 (1990-04-01), None
patent: A59500597 (1984-04-01), None
patent: A1168298 (1989-07-01), None
patent: 1-168298 (1989-07-01), None
patent: A5502888 (1993-05-01), None
patent: A1-8303103 (1983-09-01), None
patent: A1-9200993 (1992-01-01), None
Database Chemabs 'Online!, Chemical Abstracts Service, Columbus, Ohio, USA, Shimamoto, et al, “Efficient Solubilization Of Proteins Overproduced As Inclusion Bodies By Use Of An Extreme Concentration Of Glycerol”, retrieved from STN, Database accession no. 130:232959 HCA, XP-002173883, Abstract, &Tech. Tips Online (1998).

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