Method for recovering and using lignin in adhesive resins by ext

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From lignin – tannin – or derivative reactant

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

530501, 530507, 527403, C08H 502

Patent

active

050215310

ABSTRACT:
Lignin, or a lignin derived material, which has been significantly demethylated (e.g., the demethylated lignin found in the raffinate produced as a by-product of dimethyl sulfide production which can be carried out using the spent liquor from wood pulping operations) can be isolated by a process wherein an organic solvent is added to a lignin-containing aqueous solution. The organic solvent is typically a polar, and at least a partially water-immiscible substance such as, for example, ethyl acetate. The resulting lignin-containing aqueous solution/organic solvent mixture is acidified to produce a water layer which is discarded and an organic solvent layer which contains the demethylated lignin. Upon its recovery, the demethylated lignin is preferably dried and stored until it is used (along with an alkali, an aldehyde and an adhesive filler) in compounding an adhesive of the type generally used in the manufacture of plywood.

REFERENCES:
patent: 2042705 (1936-06-01), Dreyfus
patent: 2247210 (1941-06-01), Schorger
patent: 2976273 (1961-03-01), Ball et al.
patent: 3071570 (1963-01-01), Marton et al.
patent: 3227667 (1966-01-01), Moffitt et al.
Thermosetting Resins of Demethylated and Tall Oil Lignins; Khim. Ispol'z Lignina 1974:428-433.
Kraft Lignin Utilization in Adhesives; Wood Science Technology, 22:157-1-5 (1988).
Holzforschung and Holzverwertung; 30:85-87 (1978).
The Demethylation and Degradation of Lignin or Spent Liquors by Heating with Alkaline Reagents; Enkvist et al., Tappi 45:128 (1962).
Lignin-Based Wood Adhesives Nimz, Horst H., Polymer Institute, Univ. of Karlsruhe, Federal Republic of Germany.
Studies on the Effects of Methylation and Demethylation on Resin Forming Properties of Thiolignin, Smithiana, Picea; Holsforschung and Holzverwertung 30:85 (1978).
Phenol-Lignin-Formaldehyde Adhesives for Plywood; Gupta et al., Holzforschung and Holzverwertung 30(1978).
Complex Dibenzofurans; Stjernstrom, Nils; Acta Chem. Scand 16(1962) No. 3.
Proofs for the Occurrence of Homoprolocalechuic Acid and Some Other Pyrocatechol and Guaiacol Derivatives in Pressure Heated Cellulose Spent Liquors; Ashorn et al., Acta Chem. Scand. 16(1962) No. 3.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Method for recovering and using lignin in adhesive resins by ext does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for recovering and using lignin in adhesive resins by ext, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for recovering and using lignin in adhesive resins by ext will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-1027560

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.