Method for recovering alkyl vinyl ether

Details Method for recovering alkyl vinyl ether Method for recovering alkyl vinyl ether

1998-03-18

2000-07-18

Wilson, James O.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568698, 502240, 502243, 502250, 502341, C07C 4100

Patent

active

060909889

ABSTRACT:
A reaction mixture in a gas form which is obtained by intramolecular dehydration of glycol ether in a gas phase is liquidized and collected by using as a collecting agent the glycol ether which is a raw material of the reaction mixture. The collected liquid thus obtained is continuously distilled by using a continuous distillation column so that a distillate containing alkyl vinyl ether and water is obtained, while a bottom product containing glycol ether is obtained. The distillate is left to stand in a separation vessel whereby separating into an oleaginous layer and an aqueous layer, so that alkyl vinyl ether is collected as the oleaginous layer. On the other hand, in the case where the bottom product contains water, the bottom product is continuously distilled together with an azeotrope former by using a continuous distillation column whereby a distillate containing an azeotrope of water and the azeotrope former, so that glycol ether is collected as a bottom product. By doing so, a method whereby alkyl vinyl ether as well as glycol ether which is the raw material and the collecting agent are efficiently collected, purified, and recovered is realized.

REFERENCES:
patent: 5124005 (1992-06-01), Yang et al.
patent: 5650544 (1997-07-01), Ariyoshi et al.
patent: 5773669 (1998-06-01), Shimasaki et al.

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