Method for purification of phosphoric acid high purity...

Chemistry of inorganic compounds – Phosphorus or compound thereof – Oxygen containing

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C423S316000, C423S317000

Reexamination Certificate

active

06861039

ABSTRACT:
The present invention provides a purification method of phosphoric acid, which includes bringing phosphoric acid containing arsenic into contact with hydrogen halide, thereby to remove the arsenic from the phosphoric acid, and a purification method of phosphoric acid, which includes bringing phosphoric acid containing arsenic into contact with hydrogen halide in the presence of a compound capable of generating hydrogen halide under acidic conditions. According to the method for purifying phosphoric acid of the present invention, a completely new method for removing arsenic in phosphoric acid is provided, which does not require a filtration or deaeration step or shows a great amount of residual sodium, unlike a sulfide coagulation method. This method is applicable to high concentration phosphoric acid, particularly polyphosphoric acid, and can be practiced at a low cost. In addition, a conventionally nonexistent high purity polyphosphoric acid having an arsenic (As) content of not more than 1 ppm and low contents of heavy metal, silica, sodium and the like can be provided.

REFERENCES:
patent: 2287683 (1942-06-01), Hurka
patent: 3342549 (1967-09-01), Sakomura et al.
patent: 3723606 (1973-03-01), Klingelhoefer et al.
patent: 3991164 (1976-11-01), Scheibitz et al.
patent: 4044108 (1977-08-01), Kikuchi et al.
patent: 4046687 (1977-09-01), Schulze
patent: 4053564 (1977-10-01), Bradford et al.
patent: 4082836 (1978-04-01), Ore
patent: 4083934 (1978-04-01), Jernigan et al.
patent: 4215098 (1980-07-01), Lowe et al.
patent: 4296082 (1981-10-01), Lowe et al.
patent: 4309394 (1982-01-01), Hudson
patent: 4399114 (1983-08-01), Maurer et al.
patent: 4466948 (1984-08-01), Schimmel et al.
patent: 4492680 (1985-01-01), Frankenfeld et al.
patent: 4629614 (1986-12-01), Schimmel et al.
patent: 4639359 (1987-01-01), Michalski et al.
patent: 4692228 (1987-09-01), Twardowski
patent: 4777028 (1988-10-01), Schrodter
patent: 4780294 (1988-10-01), Schimmel et al.
patent: 4824650 (1989-04-01), Segrist
patent: 5246681 (1993-09-01), Calicchio
patent: 33 27 394 (1985-02-01), None
patent: 1601474 (1981-10-01), None
patent: B-53-128595 (1981-10-01), None
patent: 60-166208 (1985-08-01), None
patent: A-06-048712 (1994-02-01), None
patent: A-06-100307 (1994-04-01), None

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Method for purification of phosphoric acid high purity... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for purification of phosphoric acid high purity..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for purification of phosphoric acid high purity... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3385396

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.