Method for purification of cresidine sulfonic acid by solvent ex

Liquid purification or separation – Processes – Liquid/liquid solvent or colloidal extraction or diffusing...

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B01D 1104

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044366256

ABSTRACT:
A method for removing residual cresidine from impure p-cresidine sulfonic acid which impure p-cresidine sulfonic acid contains from above about two parts per billion to about 1500 parts per million of cresidine. The method comprises contacting an aqueous solution of the impure p-cresidine sulfonic acid with sufficient liquid hydrocarbon of from five to eighteen carbon atoms for a sufficient time to extract the cresidine from the p-cresidine sulfonic acid to a concentration of less than two parts per billion of cresidine in the p-cresidine sulfonic acid.

REFERENCES:
Dictionary of Organic Compounds, vol. 1, 1965, p. 109.
Hamilton et al., Industrial Toxicology, 1949, pp. 450-454.
Wilson et al., Textbook of-Pharmaceutical Chemistry, 1954, p. 483.

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