Method for production of maleic anhydride

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

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C549S257000

Reexamination Certificate

active

06960670

ABSTRACT:
This invention discloses a method for producing maleic anhydride comprising an azeotropic distillation step to dehydrate a crude maleic acid-containing aqueous solution, which method is characterized by as an azeotropic solvent (1) using an organic solvent exhibiting a maximum dissolving concentration of the organic solvent in water in the range of 0.1-5% by weight at a temperature of 20° C. According to this invention, it is made possible to prevent the occurrence of a blocking substance, allow a continuous operation for a long time, and remove by-produced acid components by a process of distillation for azeotropic dehydration.

REFERENCES:
patent: 2729600 (1956-01-01), Beach et al.
patent: 3357994 (1967-12-01), Popp et al.
patent: 1317308 (1961-12-01), None
patent: 41003172 (1966-02-01), None
patent: 50050316 (1975-06-01), None
patent: 03076311 (1986-02-01), None
patent: 63313782 (1988-12-01), None
patent: 05261292 (1993-10-01), None
patent: 05262754 (1993-10-01), None
patent: 05262755 (1993-10-01), None
patent: 06145160 (1994-05-01), None
Handbook of Chemistry & Physics (43rd Edition) Chemical Rubber Publ. Co., Cleveland, Ohio (1961) p. 944-945.

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