Method for producing trifluoromethanesulfonic anhydride

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfonic anhydrides group

Reexamination Certificate

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Reexamination Certificate

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07741518

ABSTRACT:
This method for producing trifluoromethanesulfonic anhydride reacting trifluoromethanesulfonic acid with phosphorus pentoxide to produce trifluoromethanesulfonic anhydride, wherein hardening of the reaction solution due to polyphosphoric acid, which is produced as a byproduct, is prevented by using an excess amount of trifluoromethanesulfonic acid with respect to the phosphorus pentoxide.

REFERENCES:
patent: 5004829 (1991-04-01), Aramaki et al.
patent: 5808149 (1998-09-01), Nakamura et al.
patent: 2-268148 (1990-11-01), None
patent: 9-227498 (1997-09-01), None
patent: 10-114734 (1998-05-01), None
patent: 11-236365 (1999-08-01), None
patent: 11-236366 (1999-08-01), None

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