Specialized metallurgical processes – compositions for use therei – Processes – Electrothermic processes
Patent
1973-12-10
1976-08-31
Hunt, Brooks H.
Specialized metallurgical processes, compositions for use therei
Processes
Electrothermic processes
75 844, C22B 5300
Patent
active
039778665
ABSTRACT:
Titanium tetrachloride is reduced at atmospheric pressure and 1245.degree.C to 1750.degree.C by molten manganese to give substantially pure molten titanium metal and gaseous manganese chloride. A counter-current stream of gaseous titanium tetrachloride contacts molten manganese to make the chlorine interchange. Titanium alloys with other metals which will not reduce titanium tetrachloride are made by adding such metals to the reactor with the molten manganese; and they end up as part of the melt with titanium. The manganese chloride formed is oxidized to the oxide while giving chlorine gas, to be used in forming the titanium tetrachloride; and the manganese oxide is carbo-thermally reduced by conventional methods to manganese metal for recycle.
REFERENCES:
patent: 2864690 (1958-12-01), Lee et al.
patent: 3004848 (1961-10-01), Hansley et al.
patent: 3043679 (1962-07-01), Campbell et al.
patent: 3058820 (1962-10-01), Whitehurst
patent: 3102807 (1963-09-01), Chisholm
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