Method for producing tetrafluoroethylene

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

Reexamination Certificate

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Details

C203S074000, C570S136000, C570S153000, C570S178000

Reexamination Certificate

active

06849163

ABSTRACT:
There is provided a process for recovering tetrafluoroethylene wherein an amount of energy required to obtain TFE is reduced.In the process for producing a TFE mixture as an intended mixture which contains TFE at a higher concentration from a raw material mixture (10) which contains TFE, a component of which boiling point is lower than that of TFE and a component of which boiling point is higher than that of TFE,(1) the raw material is subjected to a preliminary distillation treatment (12) so as to obtain (a) a first fraction (15) which contains at least a portion of the component of which boiling point is higher than that of TFE and (b) a second fraction (14) as the balance which contains TFE and the component of which boiling point is lower than that of TFE, and then(2) the second fraction is subjected to a main distillation treatment (16) so as to obtain (c) a third faction (20) formed by distilling off the component of which boiling point is lower than that of TFE, and (d) a fourth fraction (18) as the intended mixture being the balance which contains TFE.

REFERENCES:
patent: 3101304 (1963-08-01), Wiist
patent: 3221070 (1965-11-01), Okamura et al.
patent: 3834996 (1974-09-01), Also et al.
patent: 4898645 (1990-02-01), Voigt et al.
patent: 0 038 970 (1981-04-01), None
patent: 307673 (1990-02-01), None
patent: 40-18283 (1940-08-01), None
patent: 39-19624 (1964-09-01), None
patent: 4810444 (1973-04-01), None
patent: 7-233104 (1995-09-01), None

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