Method for producing sodium perborate monohydrate

Chemistry of inorganic compounds – Boron or compound thereof – Oxygen containing

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23313FB, C01B 1512

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active

054785448

ABSTRACT:
Method and apparatus for producing sodium perborate monohydrate by dehydrating sodium perborate tetrahydrate in a fluid bed with heated air. Contact surfaces are arranged inside the fluid bed whose total area is the same as up to 500 times the area of the approach-flow bottom of the fluid bed. The contact surfaces are advantageously designed as heat exchangers whose surface temperature is adjusted to maintain 90.degree. to 110.degree. C. at the contact surfaces. The method results in a sodium perborate monohydrate with especially high abrasion resistance. In addition, the energy requirement is lower than that provided in the previously known method commonly used in the industry.

REFERENCES:
patent: 3914380 (1975-10-01), Dillenburg et al.
patent: 4942025 (1990-07-01), Condo et al.
patent: 5104631 (1992-04-01), Reginato
patent: 5229092 (1993-07-01), Dugua
John H. Perry, Chemical Engineers' Handbook, Fourth Edition, McGraw-Hill Book Co. (1963), pp. 20-50 through 20-53.
Brochure of Sulzer Escher Wyss "Fliessbett-Technik" p. 10.
DIN ISO 3310 concerning seiving specimens subsequent to ball milling on cover of ISO 3310 and discussed on p. 15 of the application.
"Sodium perborates for industrial use-Determination of degree of attrition", International Standard ISO 5937, International Organization for Standardization, Nov. 1, 1980.

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