Method for producing silicon nitride molded bodies by means of p

Plastic and nonmetallic article shaping or treating: processes – Including step of generating heat by friction

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264 85, 264 86, 264332, C04B 3558, F27B 904, F27B 910

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042645468

ABSTRACT:
Method and apparatus for producing silicon nitride molded bodies by means of a pseudoisostatic hot pressing process. Silicon nitride is initially ground in a grinding vessel with grinding elements wherein the vessel is lined with the same material from which the grinding elements are made, e.g., hot pressed silicon nitride. Grinding is continued until a specific surface area greater than 15 m.sup.2 is obtained. The grinding takes place in the presence of a grinding liquid to prevent oxidation of the freshly ground silicon nitride. The silicon nitride suspension is then treated in a pressure vessel to remove the grinding liquid therefrom and form a blank. The blank is thereafter embedded within a pressure transfer medium, e.g., boron nitride, and inserted into the die of a hot pressing furnace to obtain the desired hot pressed silicon nitride.
The pressure vessel used in this method comprises a chamber for the silicon nitride suspension, an outlet means connected to the bottom of the chamber to permit the vacuum removal of the grinding fluid from said suspension; and an inlet means connected to the chamber for admitting an inert gas, e.g., nitrogen, into the chamber.

REFERENCES:
patent: 4036653 (1977-07-01), Jacobson
patent: 4112143 (1978-09-01), Adlerborn et al.
patent: 4119690 (1978-10-01), Prochazka et al.
patent: 4126653 (1978-11-01), Smith et al.
patent: 4127630 (1978-11-01), Washburn

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