Method for producing silica glass

Glass manufacturing – Processes – With measuring – sensing – inspecting – indicating – or testing

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65 32, 65 301, 264332, 423338, 501 12, 501 54, C03B 1906, C01B 3312

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043176682

ABSTRACT:
A method for producing silica glass wherein a dry silica gel subjected to a water desorption treatment and a carbon removal treatment is heated and has its temperature raised in an atmosphere containing chlorine, to perform a hydroxyl group removal treatment, the resultant silica gel is thereafter heated to a temperature of approximately 1,000.degree. C.-1,100.degree. C. in an atmosphere containing at least 1% of oxygen, to perform a chlorine removal treatment, and the resultant silica gel is further heated to a temperature of 1,050.degree. C.-1,300.degree. C. in He or in vacuum, to perform a sintering treatment. The silica glass thus produced does not form bubbles even when heated to high temperatures of or above 1,300.degree. C. Therefore, it is easily worked and it is free from the lowering of transparency attributed to the bubble formation.

REFERENCES:
patent: 4116657 (1978-09-01), Elmer
patent: 4165223 (1979-08-01), Powers
patent: 4243422 (1981-01-01), Lenz et al.
Yamane, M. et al., "Low Temperature Synthesis of a Monolithic Silica Glass by the Pyrolysis of a Silica Gel", J. Material Sciences 14 (1979), pp. 607-611.
Pastor, R. C. et al., "Crystal Growth in a Reactive Atmosphere", Mat. Res. Bull. 10 (1975), pp. 117-124.

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