Method for producing ruthenium complex

Details Method for producing ruthenium complex Method for producing ruthenium complex

2011-04-26

2011-04-26

Gonzalez, Porfirio Nazario (Department: 1621)

Organic compounds -- part of the class 532-570 series

Organic compounds

Heavy metal containing

Reexamination Certificate

active

07932411

ABSTRACT:
The present invention provides a novel method for simply and efficiently producing a ruthenium aromatic complex which is suitable also as an industrial method. The production method includes reacting a ruthenium aromatic complex with an aromatic compound as a ligand of the ruthenium aromatic complex, In a sealed reaction container at a reaction temperature higher than the boiling point of the aromatic compound to produce a ruthenium aromatic complex having, as a ligand, an aromatic compound having a lower boiling point.

REFERENCES:
Gupta et al., Organometallics, vol. 16, No. 20, pp. 4355-4361 (1997).
Gao et al., Tetrahedron letters, vol. 49, No. 42, pp. 6126-6128 (2008).
European Search Report dated Jan. 29, 2010, corresponding to European Application No. 09173619.9.
Bennett, et al., “Highly fluxional arene cyclooctatetraene complexes of zerovalent iron, ruthenium, and osmium. Single-crystal x-ray study of (cyclooctatetraene)(hexamethylbenzene) ruthenium(O), Ru(.eta.6HMB)(1-4.eta.-COT)”, Inorg. Chem. 1980, 19, 1014-1021.

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