Method for producing precipitate and catalyst

Catalyst – solid sorbent – or support therefor: product or process – Catalyst or precursor therefor – Metal – metal oxide or metal hydroxide

Reexamination Certificate

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C502S208000, C502S209000, C502S211000, C502S305000, C502S311000, C502S317000, C502S344000, C502S353000, C502S345000, C502S325000, C502S319000, C502S303000, C502S304000, C502S324000, C502S355000

Reexamination Certificate

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06867163

ABSTRACT:
A molybdenum-based precipitate is prepared according to a process including the first step of forming a crude precipitate by pH adjustment to 6.5 or less in the presence of an alkali metal compound, and the second step of dissolving the crude precipitate in aqueous ammonia and forming a precipitate by pH adjustment to 6.5 or less. Then, the resulting molybdenum-based precipitate is washed with an acid aqueous solution having a pH of 6.5 or less and containing not less than 0.01 mole/L of ammonium root. Thus, a change in average particle diameter can be suppressed and good workability can be achieved, so that a molybdenum-based precipitate having a high purity and a desired average particle diameter can be obtained.

REFERENCES:
patent: 4707460 (1987-11-01), Ishii et al.
patent: 5681973 (1997-10-01), Hoelderich et al.
patent: 32 48 600 (1984-07-01), None
patent: 44 24 625 (1996-01-01), None
patent: 63-130144 (1988-06-01), None
patent: 3-37116 (1991-02-01), None
patent: 6-287160 (1994-10-01), None
patent: 8-196908 (1996-08-01), None
patent: 2000-26123 (2000-01-01), None
U.S. Appl. No. 09/926,553, filed Nov. 19, 2001, Kuroda et al.

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