Method for producing perchloromethyl mercaptan

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07C14916

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active

039936937

ABSTRACT:
An improved process is disclosed for the manufacture of perchloromethyl mercaptan by chlorination of carbon disulfide in the presence of aqueous hydrochloric and sulfuric acids in which a high concentration of sulfuric acid is maintained in the reactor to obtain an aqueous by-product acid mixture from which sulfuric and hydrochloric acids may be separated by a simple distillation to give commercial grade hydrochloric acid and sulfuric acid.

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patent: 3673246 (1972-06-01), Meyer et al.
patent: 3808270 (1974-04-01), Rupp et al.
patent: 3865553 (1975-02-01), Masat et al.

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