Method for producing organo-metallic compounds of...

Organic compounds -- part of the class 532-570 series – Organic compounds – Heavy metal containing

Reexamination Certificate

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C556S043000, C556S046000, C556S053000, C556S058000, C556S136000

Reexamination Certificate

active

11322929

ABSTRACT:
A method for producing ferrocene and other organometallic compounds of cyclopentadiene is disclosed. Dry iron chloride (or other selected metal salt) is added to a solution of cyclopentadiene, diethylamine, potassium and dibenzo-18-crown-6 ether in a cooled flask under a dry nitrogen atmosphere. The solution is mixed vigorously for a few hours and any excess diethylamine is evaporated. Ferrocene (or other organometallic compounds of cyclopentadiene) is extracted from the residue using petroleum ether, and any solvent is removed.

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