Method for producing NF.sub.4 BF.sub.4

Details Method for producing NF.sub.4 BF.sub.4 Method for producing NF.sub.4 BF.sub.4

1976-10-12

1978-08-15

Miller, Edward A.

Chemistry of inorganic compounds

Boron or compound thereof

149119, 423351, C01B 3514

Patent

active

041072758

ABSTRACT:
SbF.sub.5 is heated in the presence of an excess of NF.sub.3 and F.sub.2 to 250.degree. C until conversion of the SbF.sub.5 to NF.sub.4 SbF.sub.6 is complete. The NF.sub.4 SbF.sub.6 may be used itself or may be combined, in 0-15 mol % excess, with CsBF.sub.4 in anhydrous HF to produce NF.sub.4 BF.sub.4.

REFERENCES:
patent: 3708570 (1973-01-01), Tolberg et al.
patent: 3980509 (1976-09-01), Lubowitz et al.
patent: 3981756 (1976-09-01), Gotzmer
Christe et al., "Inorganic Halogen Oxidizer Research," Report R-9662, pp. B1-B4 (May 2, 1975).
Goetschel et al., Inorganic Chemistry, 11, No. 7, pp. 1696-1701 (1972).

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