Method for producing nanocrystalline multicomponent and multipha

Specialized metallurgical processes – compositions for use therei – Processes – Producing or purifying free metal powder or producing or...

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264430, 264434, B22F 100, B22F 900

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057281955

ABSTRACT:
A process for producing multi-component and multiphase nanophase materials is provided wherein a plurality of elements are vaporized in a controlled atmosphere, so as to facilitate thorough mixing, and then condensing and consolidating the elements. The invention also provides for a multicomponent and multiphase nanocrystalline material of specified elemental and phase composition having component grain sizes of between approximately 1 nm and 100 nm. This material is a single element in combination with a binary compound. In more specific embodiments, the single element in this material can be a transition metal element, a non-transition metal element, a semiconductor, or a semi-metal, and the binary compound in this material can be an intermetallic, an oxide, a nitride, a hydride, a chloride, or other compound.

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Eastman, et al. "Synthesis of Nanophase Materials By Electron Beam Evaporon" NanoStructed Materials vol. 2 pp. 377-382.
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Niedzielka et al., "Nanocrystalline Aluminum-Zirconium Alloys", Engineering Foundation Conference (Mar. 12, 1994). 2 pgs.
Rittner et al., "Synthesis and Properties Studies of Nanocrystalline AL-Z1.sub.3 Zr", Scipts Metallurgies of Materials vol. 31 pp. 841-846 (May 1994) (6 pgs).
Youngdahl et al., "Synthesis of Metal-Oxide Nanocomposites", Materials Research Society (Nov. 1994) (4 pgs).

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