Method for producing hydrolysis-stable ammonium nitriles

Organic compounds -- part of the class 532-570 series – Organic compounds – Nitriles

Reexamination Certificate

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C558S378000

Reexamination Certificate

active

07005534

ABSTRACT:
The invention relates to a method for producing hydrolysis-stable ammonium nitriles by reacting a compound of formula (1), wherein R1, R2, and R3are identical or different and represent linear or branched C1–C24-alkyl groups, C2–C24-alkenyl groups, substituted or non-substituted benzyl or C1–C4-alkoxy-C1–C4-alkyl groups, or wherein R1and R2, together with the nitrogen atom to which they are bonded, form a ring with 4 to 6 C-atoms which can be substituted with C1–C5alkyl, C1–C5alkoxy, C1–C5alkanoyl, phenyl, amino, ammonium, cyano, cyanamino, chlorine or bromine and which can contain in addition to the nitrogen atom, instead of the carbon atoms, one or two oxygen or nitrogen atoms, a group N—R6or a group R3—N—R6, wherein R6 is hydrogen, C1–C5-alkyl, C2–C5-alkenyl, C2–C5-alkinyl, phenyl, C7–C9-aralkyl, C5–C7-cycloalkyl, C1–C6-alkanoyl, cyanomethyl or cyan, R4and R5are hydrogen, C1–C4-alkyl, C1–C4-alkenyl, C1–C4-alkoxy-C1–C4-alkyl, phenyl or C1–C3-alkylphenyl, preferably hydrogen, methyl or phenyl, R4especially meaning hydrogen when R5does not mean hydrogen, and X represents an anion; with an alkaline or ammonium salt of an alkane sulfonate, paraffin sulfonate, aryl sulfonate, alcohol sulfate or fatty acid alkyl carboxylate in the presence of water, at a high temperature

REFERENCES:
patent: 6498133 (2002-12-01), Borchers et al.
patent: 0 303 520 (1989-02-01), None
patent: 0 458 396 (1991-11-01), None
patent: 0 464 880 (1992-01-01), None
patent: 0 464 880 (1992-01-01), None
patent: 0 790 244 (1997-08-01), None
patent: 0 897 974 (1999-02-01), None
English abstract for EP 0790244, Aug. 20, 1997.
English abstract for EP 0897,974, Feb. 24, 1999.

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