Method for producing high-purity fluoroalkylsulfonic acid anhydr

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfonic anhydrides group

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C07F 902

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active

058081496

ABSTRACT:
The present invention relates to a method for producing a fluoroalkylsulfonic acid anhydride represented by a general formula of (C.sub.n F.sub.2n+1 SO.sub.2).sub.2 O where n is an integer ranging from 1 to 8. This method includes a step of (a) reacting diphosphorus pentoxide with a fluoroalkylsulfonic acid represented by a general formula of C.sub.n F.sub.2n+1 SO.sub.3 H where n is an integer ranging from 1 to 8, in a fluorine-containing solvent, thereby to form the fluoroalkylsulfonic acid anhydride in the fluorine-containing solvent. A fluoroalkylsulfonic acid anhydride produced by this method is high in purity and yield.

REFERENCES:
patent: 5004829 (1991-04-01), Aramaki et al.

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