Method for producing hard metal granulate

Powder metallurgy processes – Powder metallurgy processes with heating or sintering – Metal and nonmetal in final product

Reexamination Certificate

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C419S030000, C419S032000

Reexamination Certificate

active

06852274

ABSTRACT:
A hard metal granulate is produced by wet milling and spray drying in a spray tower using pure water as the liquid phase. The spray tower is configured and operated in such a way that a ratio of the quantity of water added via the slurry (in liters per hour) to tower volume (in m3) is between 0.5 and 1.8 and in that a maximum of 0.17 kg of slurry is atomized per m3of incoming drying gas. The slurry has a solid particle concentration within a range of 65-85% by weight. Under these conditions, the addition of a water-soluble, long-chain polyglycol to the slurry prior to spraying previously required in order to prevent oxidation of the hard metal granulate is no longer necessary.

REFERENCES:
patent: 4070184 (1978-01-01), Scheithauer, Jr. et al.
patent: 4397889 (1983-08-01), Benjamin et al.
patent: 5348914 (1994-09-01), Thometzek et al.
patent: 299 858 (1992-05-01), None
patent: 0 763 605 (1997-03-01), None
patent: WO 9624454 (1996-08-01), None

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