Method for producing glass preform for optical fiber

Glass manufacturing – Processes of manufacturing fibers – filaments – or preforms – Process of manufacturing optical fibers – waveguides – or...

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65DIG16, 65900, 65 174, 65416, C03B 37023

Patent

active

053644280

ABSTRACT:
A glass preform which is used for fabricating an optical fiber, has substantially no bubbles therein and contains sufficient amount of fluorine is produced by a method comprising steps of: forming a porous glass soot body from a glass-forming raw material, removing trapped gas and water from pores of the soot body by heating the soot body under pressure lower than several ten Torr. at a temperature at which the soot body is not vitrified, filling the pores of the soot body with a gas containing SiF.sub.4 and uniformly adding fluorine to the soot body, vitrifying the fluorine-added soot body into a transparent glass body, boring said transparent glass body to form a bore therein, and inserting a highly pure quartz rod in said bore to form a glass preform, or a method forming a glass soot composite body having a core portion consisting of a solid glass and a peripheral portion consisting of a porous glass mass, removing trapped gas and water from pores of the soot composite body by heating the soot composite body under a pressure lower than several ten Torr. at a temperature at which the porous glass mass is not vitrified, filling the pores in the porous glass mass of the soot composite body with a gas containing SiF.sub.4 and uniformly adding fluorine to the soot glass mass, and vitrifying the fluorine-added soot glass mass into a transparent glass mass to form a glass preform.

REFERENCES:
patent: 3868170 (1975-02-01), DeLuca
patent: 4125388 (1978-11-01), Powers
patent: 4165915 (1979-08-01), Rav
patent: 4292063 (1981-09-01), Abe
patent: 4586943 (1986-05-01), Kyoto
patent: 4629485 (1986-12-01), Berkey
patent: 4832720 (1989-05-01), Watanabe et al.
patent: 4846867 (1989-07-01), Yokoto et al.

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