Method for producing gaseous diazoalkanes

Organic compounds -- part of the class 532-570 series – Organic compounds – Diazo or diazonium

Reexamination Certificate

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C534S565000

Reexamination Certificate

active

07902342

ABSTRACT:
The invention relates to a method for producing diazoalkanes, which is characterized by dissolving a diazoalkane precursor in a first solvent, dissolving a base in a second solvent, allowing the substances to react in a reactor while forming the diazoalkane and removing the diazoxaline under reduced pressure. The inventive method is especially suitable for producing diazomethane.

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Hawley's Condensed Chemical Dictionary, 14thEdition, John Wiley & Sons, 2002, “diazomethane”.
Adamson et al., “Improved Preparations of Aliphatic Diazo-Compounds, and Certain of Their Properties”, Journal of the Chemical Society, 1551-1556, 1937.
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Adamson et al. 1937, Improved Preparations of Aliphatic Diazo-Compounds, and Certain of Their Properties, Journal of the Chemical Society. (1937).

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