Method for producing fine grained pyrolytic silicon nitride

Coating processes – Electrical product produced – Integrated circuit – printed circuit – or circuit board

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423344, 423406, C01B 2106, B05D 512

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042898013

ABSTRACT:
Novel fine grained pyrolytic silicon nitride is produced by adding a substantial amount of methane to the normal reactant gases. Silicon tetrafluoride and ammonia in ratios of 60:40 to 10:90 may be employed with additions of methane in amounts equal to from 50 to 500% of the sum of silicon tetrafluoride and ammonia. When these reactant gases are passed over a heated substrate at a low pressure pyrolytic silicon nitride with a grain size of less than about 10 microns results.

REFERENCES:
patent: 3211527 (1965-10-01), Forsyth
patent: 3226194 (1965-12-01), Kuntz
patent: 3565674 (1971-02-01), Boland et al.
patent: 3637423 (1972-01-01), Sestrich
patent: 4036653 (1977-07-01), Jacobson
patent: 4091169 (1978-05-01), Bohg et al.
patent: 4118539 (1978-10-01), Hirai et al.

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