Method for producing electronic grade...

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

Reexamination Certificate

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C564S477000, C564S479000, C564S480000, C564S497000

Reexamination Certificate

active

07825281

ABSTRACT:
A process for preparing electronics-grade 2,2′-aminoethyoxyethanol by reacting diethylene glycol with ammonia in the presence of a catalyst in a reactor to give a reaction mixture from which a crude 2,2′-aminoethoxyethanol stream is separated off and is purified further by distillation in a pure column, wherein a sidestream comprising electronics-grade 2,2′-aminoethoxyethanol is taken off from the pure column as a result of the diethylene glycol being passed through a filter which ensures a degree of removal of at least 99% for solid particles having a maximum particle size of ≦1.5 μm before the diethylene glycol is fed into the reactor, is proposed.

REFERENCES:
patent: 5288911 (1994-02-01), Koppenhoefer et al.
patent: 7183438 (2007-02-01), Gerlach et al.
patent: 2008/0255351 (2008-10-01), Hoffer et al.
patent: 0510382 (1992-10-01), None
patent: WO-03/076386 (2003-09-01), None
patent: WO-2007/036496 (2007-04-01), None
patent: WO 2008/037587 (2008-04-01), None
patent: WO 2008/037589 (2008-04-01), None
patent: WO 2008/037590 (2008-04-01), None
Database CAPLUS on STN, Acc. No. 1977:75586, Koliushko et al., Gazovaya Promyshlennost (1976), 8, p. 25-27 (abstract).

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