Method for producing ditrimethylolpropane

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

Reexamination Certificate

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C568S699000

Reexamination Certificate

active

07553994

ABSTRACT:
In the method of producing ditrimethylolpropane of the present invention, the distillation still residue obtained in the production of trimethylolpropane is subjected to crystallizing treatment while strictly regulating the amount of organic solvent to be used, the crystallization temperature and the crystallization time within the specific ranges. With the method of the present invention, a highly pure di-TMP is obtained only by a single operation of the crystallization.

REFERENCES:
patent: 3740322 (1973-06-01), Wada et al.
patent: 3829507 (1974-08-01), Zey
patent: 2002/0033325 (2002-03-01), Ninomiya et al.
patent: 1178030 (2002-02-01), None
patent: 1292405 (1972-10-01), None
patent: 2002-047231 (2002-02-01), None
patent: 2002-047232 (2002-02-01), None
Communication and European Search Report dated Dec. 11, 2004, for No. EP 04 01 3343.

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