Method for producing deuterated methyl methacrylate

Details Method for producing deuterated methyl methacrylate Method for producing deuterated methyl methacrylate

2008-05-20

2008-05-20

Eyler, Yvonne (Department: 1621)

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acid esters

Reexamination Certificate

active

07375247

ABSTRACT:
A method for producing MMA-d8which includes a step of exchanging D in hydroxyl group of methanol-d4represented by the formula: CD3OD with H to prepare the methanol-d3represented by the formula CD3OH and simultaneously recovering a deuterium-containing compound, and a step of reacting methanol-d3with sulfuric acid salt of methacrylic acid amide represented by the formula CD2=(CD3)CO(NH2.H2SO4) to prepare MMA-d8represented by the formula: CD2=(CD3)COOCD3.

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