Chemistry of inorganic compounds – Sulfur or compound thereof – Oxygen containing
Patent
1994-08-01
1995-08-08
Langel, Wayne
Chemistry of inorganic compounds
Sulfur or compound thereof
Oxygen containing
C01B 1798
Patent
active
054396638
ABSTRACT:
This invention relates to a process for producing Caro's acid by reaction of at least 85% by weight sulfuric acid and at least 50% by weight hydrogen peroxide wherein the sulfuric acid and hydrogen peroxide are fed through separate feed lines into a funneling zone open to the atmosphere, the feed lines having air gaps between their ends and the funneling zone; continuing to introduce the sulfuric acid and the hydrogen peroxide into the funneling zone to flow and mix within the funneling zone, passing the resulting mixture by gravity flow into one end of a reaction zone whose size permits a pressure drop which is at least 8 times the theoretical pressure drop for such reaction zone and removing a mixture containing Caro's acid from the exit end of the reaction zone.
REFERENCES:
patent: 2789954 (1957-04-01), Fell
patent: 2926998 (1960-03-01), D'Addieco et al.
patent: 3900555 (1975-08-01), Jourdan-LaForte
patent: 3939072 (1976-02-01), LaForte
patent: 4915849 (1990-04-01), Griffiths et al.
patent: 5141731 (1992-08-01), Meier et al.
patent: 5304360 (1994-04-01), Lane et al.
Carmichael James
Manganaro James L.
Sacks Martin E.
Baker Patrick C.
FMC Corporation
Ianno Frank
Langel Wayne
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