Method for producing an essentially chlorite-free, stable...

Liquid purification or separation – Processes – Chemical treatment

Reexamination Certificate

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C210S764000, C210S167110, C423S477000

Reexamination Certificate

active

10480009

ABSTRACT:
The invention relates to a method for producing an essentially chlorite-free, stable, aqueous chlorine-oxygen solution. Said method comprises the following steps: (1) a hydrogen sulfate compound is dissolved in water, (2) an acid is added to the aqueous solution containing hydrogen sulfate in such a quantity that the pH value in the target final product in the form of the essentially chlorite-free, stable, aqueous chlorine-oxygen solution is maintained between approximately 3 and 5; (3) a peroxide compound is added; and (4) an aqueous chlorite solution is added dropwise in a quantity of between approximately 60 and 90 mole %, especially between 70 and 80 mole %, of chlorite, in relation to the concentration of peroxide compound. The invention also relates to the chlorine-oxygen solutions which can be obtained by means of said method.

REFERENCES:
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patent: 4296103 (1981-10-01), Laso
patent: 4574084 (1986-03-01), Berger
patent: 4725437 (1988-02-01), Kuhne
patent: 5009875 (1991-04-01), Kelley et al.
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G. Gordon Is all Chlorine Dioxide Created Equal? XP 008009991, pp. 163-174,Apr. 2001.
Umwelt und Degussa, XP 000847684, Jul. 1999.

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