Method for producing an aqueous hydroxylamine solution...

Distillation: processes – separatory – Distilling to separate or remove only water – From organic compound

Reexamination Certificate

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C203S036000, C203S037000, C203S099000, C203SDIG019, C423S387000

Reexamination Certificate

active

07105078

ABSTRACT:
A process for preparing a salt-free aqueous hydroxylamine solution by reacting an aqueous solution of a hydroxylammonium salt with a base to give a mixture and separating from said mixture by distillation a salt-free aqueous hydroxylamine solution, involving using as a base an aqueous solution of a mixture of NaOH and KOH in a molar ratio Na+:K+in the range from 70:30 to 95:5 and with a total concentration of Na+and K+in the range from 0.1 to 10 m/m % based on the total amount of the mixture.

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Gefaehrliche Chemische Reaktionen 25, Stoffinformationen, Hydroxylamin, 1984.

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