Method for producing alkylpolyalkylene glycol esters of...

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters

Reexamination Certificate

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Reexamination Certificate

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06872848

ABSTRACT:
Alkylpolyalkylene glycol esters of monoethylenically unsaturated carboxylic acids are prepared by esterifying (a) monoethylenically unsaturated carboxylic acids with (b) polyalkylene glycols which are endcapped at one end, in the absence of a solvent and in the presence of polymerization inhibitors and esterification catalysts at not more than 160° C. by a process in which the esterification is first carried out under atmospheric pressure or at up to 50 bar, the water formed in the esterification is then distilled from the reaction mixture at from 10 to 500 mbar and the esterification is then continued under atmospheric pressure or at up to 50 bar.

REFERENCES:
patent: 5037978 (1991-08-01), Mirabelli
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patent: 0 989 108 (2000-03-01), None
patent: 0 989 109 (2000-03-01), None
patent: 1 090 901 (2001-04-01), None
patent: 1090901 (2001-04-01), None

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