Method for producing acrylic fiber precursors

Plastic and nonmetallic article shaping or treating: processes – Carbonizing to form article – Filaments

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264 296, 264 297, 264 83, 264182, 264206, 2642102, 2642103, 2642105, 2642107, 2642108, 26421115, 26421117, 264232, 264233, 2642356, 264346, 4234474, 4234476, 4234478, 4234477, D01F 922

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046954155

ABSTRACT:
An acrylic fiber precursor for high performance carbon fibers free of defects which comprises an acrylonitrile polymer containing at least 90% by weight of acrylonitrile and has a surface roughness of 2.0 to 3.0 with dense inner structure. from a solution comprising 24 to 27.5% of the acrylonitrile polymer is dry-jet wet spun into a coagulation bath consisting essentially of dimethylformamide or dimethylacetamide and having a bath temperature of 5.degree. to 25.degree. C.Carbon fibers obtained by carbonizing these precursor acrylic fibers have no fusion bonding or agglutination of filaments and exhibit high performance.

REFERENCES:
patent: 3558761 (1971-01-01), Tobara et al.
patent: 3636187 (1972-01-01), Ohfuka et al.
patent: 3673035 (1972-06-01), Whitney
patent: 3814739 (1974-06-01), Takeda

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