Method for producing a silica mask on metal oxide surface

Coating processes – Heat decomposition of applied coating or base material

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427248, 427256, 427272, 427273, 427282, B05D 302

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active

054664837

ABSTRACT:
A method for producing a silica mask on metal oxide surface is disclosed. Benzaldehyde is adsorbed on neutral or weak alkaline metal oxide surface, and then tetra-methoxy silane is deposited. The tetra-methoxy silane is hydrolyzed by water vapor into silica and the adsorbed benzaldehyde is removed by NH3 as benzo-nitrile. Thus a silica mask is produced on the metal oxide surface, and the mask has vacancies corresponding to the removed benzaldehyde. The vacancies act as the adsorption sites for shape selective adsorption.

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patent: 4332837 (1982-06-01), Peyre-Lavigne
Niwa et al., Applied Catalysis, "Benzaldehyde-amminia titration method for discrimination between surfaces of metal oxide catalysts", 67 (1991) pp. 297-305.
The Proceeding of 72th Catalyst Conference (A), Sep. 28-30, 1993.

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