Method for producing 5-nitro-2-furfuryl acetate

Details Method for producing 5-nitro-2-furfuryl acetate Method for producing 5-nitro-2-furfuryl acetate

1975-08-18

1977-08-30

Jiles, Henry R.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D30770

Patent

active

040454533

ABSTRACT:
Furfuryl acetate is reacted at 0.degree.-20.degree. C with a mixture containing strong nitric acid and less than 7 mole, preferably less than 5 mole, acetic anhydride per 1 mole furfuryl acetate, in order to produce an intermediate of nitration, whereafter water is added and the aqueous solution is neutralized to a pH of 4.7-6.5 and finally the mixture is heated to 40.degree.-60.degree. C.

REFERENCES:
patent: 2490006 (1949-11-01), Kimel et al.

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