Food or edible material: processes – compositions – and products – Inhibiting chemical or physical change of food by contact... – Biocidal or disinfecting chemical agent
Reexamination Certificate
2001-08-02
2003-08-26
Sayala, Chhaya D. (Department: 1761)
Food or edible material: processes, compositions, and products
Inhibiting chemical or physical change of food by contact...
Biocidal or disinfecting chemical agent
C426S535000, C426S547000, C426S807000
Reexamination Certificate
active
06610341
ABSTRACT:
FIELD OF THE INVENTION
The present invention relates to a method for preserving processed grains, such as steam-flaked or steam-rolled grains, and to animal feed comprising the same, and optionally also comprising molasses, by use of alkali metal sulfite, bisulfite, metabisulfite or mixtures.
BACKGROUND OF THE INVENTION
The use of sulfite containing additives to preserve food by scavenging oxygen has long been known, as described in various issued patents, e.g., U.S. Pat. No. 2,799,583 (Harris), U.S. Pat. No. 2,825,651 (Loo et al), U.S. Pat. No. 3,169,068 (Block) and U.S. Pat. No. 3,284,212 (Tribble).
Prior art uses of sodium metabisulfite for silage preservation purposes, such as is described in the above-noted Harris patent, have primarily been concerned with the preservation of silages through removal of oxygen to inhibit spoilage based on the growth of oxygen-dependent mold or bacteria, as part of a fermentation cycle of fresh harvested forage stored on a farm site.
Harris describes a process for the preservation of silage, which may include unprocessed grain, by the addition of an alkaline metabisulfite and urea. The urea is present to control the corrosivity of the metabisulfites toward ferrous metals used in the construction of silos. The proportion of metabisulfite is said, by Harris, not to be critical and is said to vary from about 0.1 to 1.0%, by weight, or from 2-20 lbs/ton of silage.
On the contrary, as will be described more fully below, the process and compositions of this invention is concerned with processed grains, such as steam-flaked or steam-rolled grains and others as described below, and/or animal feed comprising such grains, and optionally molasses, and to prevention of mold and yeast growth in the animal feed. These grains or feed are not intended for a fermentation process of any kind.
U.S. Pat. No. 3,184,314 describes preservation and controlling of fermentation of high moisture content grain silages by the use of compositions comprising (a) and alkali or alkaline earth metal sulfate salt, and (b) an amylolytic enzyme, preferably malt diastase.
In U.S. Pat. No. 4,508,737, it was found that superior, fast acting preservation of and fermentation control for various silages and stored grains, especially high moisture content grains, can be provided by use of 0.2-1.5 lbs of alkali metal sulfite, alkali metal bisulfite, alkali metal metabisulfite or mixtures thereof.
In both U.S. Pat. No. 3,184,314 and U.S. Pat. No. 4,508,737, fermentation control was the key factor for adequate preservation of fresh harvested forages on the farm.
It has now been found in the present invention that preservation during the storage of animal feeds, particularly commercially manufactured animal feeds, such as cattle feed, swine feed, poultry feed, horse feeds, and pet feed, comprising processed grains and optionally molasses, can be achieved by applying the compositions of this invention during the manufacturing process, either directly onto the grain, into the total feed mix, and/or into the added molasses.
The use of propionic acid usually about 1-2% by weight of processed grains has gained wide acceptance. While this method is effective for inhibiting microbial growth, grains treated with these large amounts of propionic acid are often unacceptable when it comes to odor and palatability to the animal, denoted by reduced intake by animals. Industry practice is to use less than 1% propionic acid with the result of solving only partially the problem of moldy animal feed.
SUMMARY OF THE INVENTION
The invention relates to the preservation of animal feed, particularly commercially produced animal feed, such as cattle feed, horse feed, swine feed, poultry feed or pet (e.g., dog, cat, or bird) feeds, which comprise processed grains, such as steam-flaked grains or steam-rolled grains, and others as described below and optionally molasses.
In order to provide palatable animal feed, free from tastes or odors which would discourage feeding and still retain a high proportion of nutrient and vitamin values, it has been found to be essential to stop undesired oxygen-dependent mold and yeast growth as quickly as possible during the manufacturing process, and continuing such preservation during a reasonable period, 30-45 or more days for example, when such feed is in commercial warehouse storage waiting to be distributed for final feeding to animals.
The present composition achieves this dual result in a uniquely effective way by adding from about 0.1 to 2 lbs/ton of processed grain, of an alkali metal sulfite, bisulfite, metabisulfite or mixtures thereof. If the amount is below about 0.05 lbs/ton, the effect is inadequate to produce the desired mold control effect. Sulfite amounts at the lower end of the range have been found particularly effective with a sulfite amount of 0.1 to 1.5 lbs/ton of processed grain. Preferably, the amount of said compound is in the range of from 0.1 to 0.8 lbs/ton of processed grain.
The compositions may be applied directly to the processed grains or in the total feed mix in any known manner practical for production runs; as for example, by preparing the composition in a liquid aqueous solution and spraying the solution or formulating the composition in dry granular form and applying at the point most appropriate in the manufacturing procedure, after the grain has been processed, assuring thorough coverage.
The compositions are particularly effective in reducing mold and yeast growth on the processed grain, such processed grains being defined as follows: grain already dried at 10-12% moisture undergo a variety of processes which crack the hull or remove the hull from the grain, exposing the internal nutrients of the grain. Such processes, including but not limited to those described below, are required by manufacturers to make such grains usable for the production of animal feed, causing exposure of grain nutrients to additional moisture thereby causing problems with mold and yeast growth during storage in factory bins while awaiting production runs, storage time being from a few hours to a few days.
Commonly used processes include steam-flaking or steam-rolling at high temperatures in excess of 200° F., the final moisture being 14-16% when coming out of the cooler system; groats (de-hulled grain), as well as cracked, crimped or ground grain, which although not exposed to additional steam and heat, contain exposed nutrients of the grain which absorb sufficient moisture during the storage and feed mixing processes, causing mold problems in the final feed. Processed grains also include the by-products of processed grains by the food industry which are purchased by the manufacturers of animal feed, such as grain hulls, and granular particles known as middlings, which are rejected by the flour processing industry, such by-products containing hulls or various granular size grain particles, which are often used in animal feeds as a filler or a fiber source to arrive at a total final feed mixture.
Applying the present composition directly on the processed grains, or in the feed mix or to added molasses significantly reduces the mold and yeast growth during the manufacturing process.
Additionally, preservation with the present composition continues to be uniquely effective during normal storage conditions after the totally mixed animal feed leaves the factory, packaged in 50-pound bags or is stored in bulk bins until it is finally fed to the animal. Curbing mold and yeast growth is the key factor in keeping such feed nutritious and fresh for animal consumption.
DETAILED DESCRIPTION OF THE INVENTION
The use of certain effective amounts of alkali metal sulfite, bisulfite, metabisulfite or mixtures thereof have been discussed in the present invention to permit both effective protection of the processed grains and/or total feed mixes from the effects of the growth of aerobic molds, and also contributes to the desired preservation of fresh consumable feed. Effective amounts of the alkali metal sulfite, bisulfite or metabisulfite are from about 0.1 to 2 lbs/ton of process
International Stock Food Corporation
Sayala Chhaya D.
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