Method for preparing titanium diboride shapes

Plastic and nonmetallic article shaping or treating: processes – Including step of generating heat by friction

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106 733, C04B 3558

Patent

active

042750261

ABSTRACT:
Cold formed and sintered titanium diboride shapes of high density are prepared by grinding particulate carbothermic titanium diboride in a mill having non-contaminating grinding media in the presence of an inert, substantially oxygen-free liquid grinding aid to form finely-divided titanium diboride powder having a surface area of at least about 3 square meters per gram, cold forming the finely-divided titanium diboride powder into a desired shape and sintering the shape to produce a titanium diboride article having a density of at least 95 percent of the theoretical density of titanium diboride.

REFERENCES:
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patent: 2802748 (1957-08-01), Glaser
patent: 3003885 (1961-10-01), Mandorf
patent: 3028324 (1962-04-01), Ransley
patent: 3052538 (1962-09-01), Jech et al.
patent: 3215545 (1965-11-01), Reidl et al.
patent: 3314876 (1967-04-01), Ransley
patent: 3937619 (1976-02-01), Clougherty
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patent: 4017426 (1977-04-01), Carbonnel
patent: 4097567 (1978-06-01), Cebulak et al.
patent: 4108670 (1978-08-01), Steiger et al.
Sintering and Recrystallization of ZRC-ZRB.sub.2 Compacts by V. M. Gropyanou et al., Soviet Powder Metallurgy, Jul. 1968.

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