Method for preparing ticrynafen

Details Method for preparing ticrynafen Method for preparing ticrynafen

1977-08-22

1978-08-15

Siegel, A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D33324

Patent

active

041071794

ABSTRACT:
A new method for preparing ticrynafen comprises reacting 2,3-dichloro-4-hydroxyphenyl-2-thienylmethanone with an alkali metal salt of chloro or bromo acetic acid in aqueous solvent. An advantageous aspect of the reaction is that yields are increased with the addition of an alkali metal iodide to the reaction mixture.

REFERENCES:
patent: 3758506 (1973-09-01), Godfroid
patent: 4017632 (1977-04-01), Thuillier

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