Method for preparing shaped, green ceramic compacts

Plastic and nonmetallic article shaping or treating: processes – Including step of generating heat by friction

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106 63, 264 61, 264176R, 264DIG25, C04B 3564

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active

040201341

ABSTRACT:
A method for preparing shaped, green ceramic compacts suitable for firing to form high density .beta."-alumina containing ceramic bodies comprising: (1) mixing between about 2.5 parts by weight and about 4.5 parts by weight of a ceramic composition comprising at least about 80 weight percent of aluminum oxide and from about 5 to about 15 weight percent of sodium oxide with 1 part by weight of a binder composition consisting essentially of between about 20 weight percent and about 35 weight percent of polyvinyl pyrrolidone having a number average molecular weight (M.sub.n) between about 20,000 and about 160,000 and between about 80 weight percent and about 65 weight percent of ethylene glycol; (2) extruding the mixture so formed through a die of desired configuration; and (3) heating the extrudate at temperatures and for periods of time necessary to evaporate the ethylene glycol solvent and burn off the polyvinyl pyrrolidone.

REFERENCES:
patent: 2952877 (1966-09-01), Park
patent: 3285873 (1966-11-01), Bailey
patent: 3417054 (1968-12-01), Merijan et al.
patent: 3652749 (1972-03-01), Sobel et al.
Bruch, "Extruding Fine Alumina Powders," Ceramic Age, June (1972), pp. 18-25.

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