Method for preparing samples for microscopic examination

Etching a substrate: processes – Adhesive or autogenous bonding of two or more...

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216 39, 216 52, 216 60, 216 66, 216 85, 438 8, 438691, 438745, B44C 122, H01L 2100

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060427361

ABSTRACT:
The present invention provides a method for preparing samples for microscopic examination that requires a glass slide to be laminated to a sample substrate by an adhesive layer for polishing in a sample polishing process. A cavity can be first formed in the surface of the substrate by a focused ion beam technique to reveal a characteristic feature which needs to be examined. A wax-based material is then used to fill the cavity and to protect the characteristic feature before an adhesive layer is applied on top of the substrate for bonding a glass slide to the substrate. After the sample is sectioned in the polishing process to reveal a new cross-section that contains the characteristic feature, the protective coating of the wax-based material can be removed by a suitable solvent such that the characteristic feature is ready for microscopic examination. A suitable wax-based material can be a wax that is similar to a candle wax which can be easily removed by acetone.

REFERENCES:
patent: 4389280 (1983-06-01), Mueller et al.
patent: 5064498 (1991-11-01), Miller
patent: 5662814 (1997-09-01), Sugino

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