Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters
Patent
1997-08-13
1999-02-02
Geist, Gary
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acid esters
C07C 6952
Patent
active
058667130
ABSTRACT:
A method for preparing a (meth)acrylic acid ester, which comprises reacting (meth)acrylic acid with a C.sub.1-3 alcohol in the presence of a strongly acidic ion exchange resin as a catalyst, wherein the reaction is carried out under reduced pressure while the molar ratio of the alcohol to the (meth)acrylic acid is adjusted to be less than 1, whereby it is possible not only to improve the esterification yield by one pass but also to reduce the amount of a by-product alkoxypropionate which is problematic in the purification system.
REFERENCES:
patent: 4250328 (1981-02-01), Fujita et al.
patent: 4435594 (1984-03-01), Matsumura et al.
Mine Norioki
Sugimoto Chikara
Suzuki Yoshiro
Yamagishi Masahiko
Geist Gary
Mitsubishi Chemical Corporation
Parsa Jafar
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