Method for preparing dexchlor tannate

Drug – bio-affecting and body treating compositions – Designated organic active ingredient containing – Carbohydrate doai

Reexamination Certificate

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Details

C514S025000, C514S649000, C514S279000, C514S299000, C514S850000, C536S001110, C536S004100, C536S119000, C536S124000, C560S068000

Reexamination Certificate

active

06939856

ABSTRACT:
The invention pertains to a method for preparing dexchlorpheniramine (“dexchlor”) tannate by reacting dexchlorpheniramine free base at a temperature of about 75 to about 150° C. with tannic acid neat or as an aqueous slurry containing up to about 20 wt. % water. The dexchlorpheniramine free base may be obtained by reacting a commercially available dexchlorpheniramine salt such as dexchlorpheniramine maleate with a base such as aqueous sodium hydroxide. The resultant dexchlor tannate has extended release properties and is useful in pharmaceutical compositions as an antihistamine for human beings.

REFERENCES:
patent: 3061517 (1962-10-01), Watter
patent: 3282789 (1966-11-01), Marty et al.
patent: 5599846 (1997-02-01), Chopdekar et al.
patent: 5663415 (1997-09-01), Chopdekar et al.
patent: 6037358 (2000-03-01), Gordziel
patent: 6287597 (2001-09-01), Gordziel
patent: 6306904 (2001-10-01), Gordziel
patent: 6509492 (2003-01-01), Venkataraman
patent: WO 02/05745 (2002-01-01), None
patent: WO 02/05746 (2002-01-01), None
patent: WO 02/05747 (2002-01-01), None

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