Method for preparing dense tungsten ingots

Powder metallurgy processes – Powder metallurgy processes with heating or sintering – Powder shape or size characteristics

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419 26, 419 39, 419 49, 419 68, 75248, B22F 100

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049717570

ABSTRACT:
Dense tungsten ingots are prepared by hot isostatically pressing at a temperature of about 1500.degree. to about 1700.degree. C. and a pressure of about 20 to about 30 ksi for about 2 to about 3 hours a refractory container comprising a green tungsten metal compact in contact with a dopant, the tungsten metal of the compact being formed prior to contact with the dopant; the dopant being a material which is insoluble in tungsten and contains molecules having atomic radii greater than the atomic radius of tungsten by at least about 15%.

REFERENCES:
patent: 4458599 (1984-07-01), Mullendose et al.
patent: 4801330 (1989-01-01), Bose et al.
"Cold Isostatic Pressing of Metal Powders", Metals Handbook, 9th Edition, vol. 7, pp. 444-450.
Application Ser. No. 364,388, filed Jun. 12, 1989.
Kirk-Othmer, Encyclopedia of Chemical Technology, Third Edition, vol. 20, pp. 38-64.
Metals Handbook, 9th Edition, vol. 7, p. 6.
Metals Handbook, "Hot Isostatic Pressing of Metal Powders", 9th Edition, vol. 7, pp. 419-443.

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