Method for preparing carborane

Details Method for preparing carborane Method for preparing carborane

1976-05-28

1978-03-28

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 502

Patent

active

040814840

ABSTRACT:
Improved yields of n-hexyl carborane are obtained by slowly adding an ether solution of decaborane and dialkylsulfide to 1-octyne at a temperature between about 110.degree. and 140.degree. C.

REFERENCES:
patent: 3463820 (1969-08-01), Ager et al.
patent: 3505409 (1970-04-01), Bobinski et al.
Heying et al., Inorg. Chem. 2, pp. 1089-1092 (1963).
Hill et al., Inorg. Chem. 14, pp. 1244-1249 (1975).
Fein et al., Inorg. Chem. 2, pp. 1111-1119 (1963).
Chemical Abstracts, 80, 37268w (1974).

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