Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1986-06-03
1988-09-13
Killos, Paul J.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07C 5803
Patent
active
047708212
ABSTRACT:
There is provided a method for preparing .beta.-chloropivaloyl chloride which includes chlorinating pivalic acid to form pivaloyl chloride and reacting the resultant pivaloyl chloride with a chlorine gas in a gaseous phase to form .beta.-chloropivaloyl chloride. Both steps may be carried out by a continuous process or a batch process. According to this method, the chlorination in the second step can be achieved at a low temperature, and the formation of by-products is reduced and production efficiency can be enhanced.
REFERENCES:
Groggins, P. H. Unit Processes in Organic Synthesis, 5th Ed. (1958) McGraw-Hill, publ., pp. 212 222-226.
Furusawa Osamu
Miyazawa Kenichi
Ihara Nikkei Chemical Industry Co., Ltd.
Killos Paul J.
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