Plastic and nonmetallic article shaping or treating: processes – Vacuum treatment of work – To degas or prevent gas entrapment
Reexamination Certificate
2000-10-04
2003-04-15
Ortiz, Angela (Department: 1732)
Plastic and nonmetallic article shaping or treating: processes
Vacuum treatment of work
To degas or prevent gas entrapment
C264S135000, C264S250000, C264S271100, C264S319000, C264S294000
Reexamination Certificate
active
06547998
ABSTRACT:
The invention relates to a method for preparation of test bodies for analysis of porous, preferably thermally sprayed, surface layers which are incorporated by casting in plastic.
To be able to analyze thermally sprayed surface layers, so called test bodies have to be produced, which are lapped and examined and evaluated with the use of a microscope with regard to the structure of the surface layer. It is when the test body is lapped that the problem arises in that the surface layer is “smeared out”, which will give a false structure.
There are two known methods for incorporating by casting of test bodies, viz. on one hand a cold casting method and on the other hand a warm casting method, which will be described below.
In the cold casting method, test bodies are produced by incorporating by casting a test piece under vacuum in a specific two-component resin of epoxy type with very good penetration ability into porous layers, i.e. the surface of the test pieces are wetted very well. Since the epoxy resin will fill out all pin-holes and voids in the surface layer, said surface layer can be lapped after curing the epoxy resin with a very good result without any smearing of said surface layer, whereby a true structure is obtained which can be evaluated with use of a microscope.
This method suffers from the drawbacks that on one hand the curing time for the epoxy system used at room temperature amounts to several hours and that on the other hand the epoxy resin used is very expensive, which means that the costs can be very high at a large number of tests.
In the other method, i.e. the hot casting method, test bodies are produced in the way that a sample of the surface layer is incorporated by casting in a pulverized phenolic plastic, preferably bakelite, at a pressure of about 5-15 kN and a temperature of about 150° C. in a so called Pronto-press. This method has the advantage that the incorporation by casting is very fast, about 15 minutes, and that the cost per body is very low. However, the drawback is that the bakelite does not penetrate into the pin-holes and voids in the porous surface layer, whereby the result of the lapping of the surface layer is non-useable, since there is a great risk for “smearing” of the surface layer, which will produce a false structure.
The object of the invention is to eliminate the drawbacks of the above-mentioned methods.
This is achieved according to the invention by:
a) placing one or more test pieces of the surface layer in a mould introduced into a vacuum chamber, the pressure of which is lowered,
b) pouring a ready-mixed, liquid casting resin into the mould containing the test pieces,
c) again letting the air into the chamber,
d) lifting the test pieces out of the casting resin and allowing excess of casting resin to drip from the test pieces, and after that they are placed in a mould cavity of a hot moulding press,
e) filling said mould cavity together with the test pieces with a pulverized resin, and
f) applying pressure and heat to the mould cavity for a predetermined period of time, whereupon the test body is ready to be taken out and lapped.
A non-limiting example of the invention will now be described with reference to the accompanying drawing, which shows the structure of a ready-made test body with sprayed layers incorporated by casting with the method according to the invention.
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Dickstein , Shapiro, Morin & Oshinsky, LLP
Ortiz Angela
Volvo Aero Corporation
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