Method for performing the purifying separation of crystals...

Chemistry: physical processes – Physical processes – Crystallization

Reexamination Certificate

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C023S296000, C062S532000, C062S540000, C062S542000, C062S544000, C210S774000, C422S245100, C422S252000, C562S598000, C562S600000, C585S812000

Reexamination Certificate

active

07540884

ABSTRACT:
A process for purifying removal of crystals from their suspension in mother liquor by means of a washing column having forced transport in which the process chamber is encased by a metal wall which, on its side facing away from the process chamber, is heated at least along the length of the pure melt zone.

REFERENCES:
patent: 2747001 (1956-05-01), Weedman et al.
patent: 2765921 (1956-10-01), Green et al.
patent: 2851368 (1958-09-01), Findlay et al.
patent: 2854494 (1958-09-01), Thomas et al.
patent: 2912469 (1959-11-01), Wiegandt
patent: 3222880 (1965-12-01), Findlay
patent: 3261170 (1966-07-01), McCarthy et al.
patent: 3375082 (1968-03-01), Roderich
patent: 3770386 (1973-11-01), Hayashi et al.
patent: 3777892 (1973-12-01), Thijssen et al.
patent: 3872009 (1975-03-01), Thijssen
patent: 4279130 (1981-07-01), Finch et al.
patent: 4453959 (1984-06-01), Bishkin
patent: 4597768 (1986-07-01), Thijssen et al.
patent: 4632809 (1986-12-01), Otto et al.
patent: 5090965 (1992-02-01), Kehm et al.
patent: 7112695 (2006-09-01), Eck et al.
patent: 2003/0060661 (2003-03-01), Eck et al.
patent: 535 058 (1973-03-01), None
patent: 100 17 903 (2001-10-01), None
patent: 100 36 880 (2002-02-01), None
patent: 100 36 881 (2002-02-01), None
patent: 0 083 463 (1983-07-01), None
patent: 0 097 405 (1984-01-01), None
patent: 0 098 637 (1984-01-01), None
patent: 0 305 316 (1989-03-01), None
patent: 0 398 437 (1990-11-01), None
patent: 01/77056 (2001-10-01), None
P.J. Jansens, et al. “The purification process in hydraulic packed-bed wash columns”, Chemical Engineering Science, vol. 50, No. 17, pp. 2717-2729 1995.
D. Verdoes, et al. “Improved procedures for separating crystals from the melt”, Applied Thermal Engineering , vol. 17, Nos. 8-10, pp. 879-888 1997.
Letter of Rene Klomp (Niro Process Technology) to Mr. Baumann (BASF), dated May 11, 1999.
Brochure, “Crystallization and wash column separation set new standards in purity of chemical compounds,” Niro Process Technology B. V., Nov. 27, 2006, pp. 1-6.
McKay, D. L., et al., “Continuous fractional crystallization,” Chemical Engineering Progress, vol. 61, No. 11, Nov. 1965, pp. 99-104.
Oord-Knol, L. V., “Hydraulic Wash Columns Solid-Liquid Separation in Melt Crystallization,” Universal Press, 2000, ISBN 9080570915, pp. 22-24.
Arkenbout, G. F., “Melt Crystallization Technology,” Technomic Publishing Co., 1995, ISBN 1566761816, pp. 271-277.
Perry's Chemical Engineer Handbook, 7thEd. (ed. R. H. Perry, D. W. Green), McGraw-Hill Professional, 1997, ISBN 0070498415, pp. 10-133-10-137.
Verdoes, D. et al., “Comparison of Melt Crystallization Processes for the Purification of Caprolactam,” Proceeding of the 13thSymposium on Industrial Crystallization, Sep. 16-19, 1996, pp. 767-772.
Jansens, P. J., “Fractional Suspension Crystallization of Organic Compounds,” Universal Press, 1994, ISBN 9037000975, pp. 60, 126-129, 138-144, and 148.
Fax letter of Mr. Ray Ruemekorf (Niro Process Technology) to Mr. Baumann, dated Jun. 22, 1999.
Declaration of Mr. Ray Ruemekorf, Nov. 22, 2006.

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