Method for measuring recovery of catalytic elements from...

Chemistry: analytical and immunological testing – Testing of catalyst

Reexamination Certificate

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C436S079000, C436S080000, C436S084000, C436S166000, C436S172000, C436S173000, C436S174000, C356S316000, C356S318000, C250S288000

Reexamination Certificate

active

07901940

ABSTRACT:
A method is provided for measuring the concentration of a catalytic clement in a fuel cell powder. The method includes depositing on a porous substrate at least one layer of a powder mixture comprising the fuel cell powder and an internal standard material, ablating a sample of the powder mixture using a laser, and vaporizing the sample using an inductively coupled plasma. A normalized concentration of catalytic element in the sample is determined by quantifying the intensity of a first signal correlated to the amount of catalytic element in the sample, quantifying the intensity of a second signal correlated to the amount of internal standard material in the sample, and using a ratio of the first signal intensity to the second signal intensity to cancel out the effects of sample size.

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